A Small Scale Approach to Organic Laboratory Techniques (4th Edition)

Solutions and explanations
A Separation and Purification Scheme
Infrared Spectroscopy and Boiling-Point Determination
Acetylsalicylic Acid
TLC Analysis of Analgesic Drugs
Isolation of Caffeine from Tea Leaves
Isopentyl Acetate (Banana Oil)
Isolation of Eugenol from Cloves
Spearmint and Caraway Oil: M-and (-)-Carvones
Isolation of Chlorophyll and Carotenoid Pigments from Spinach
Ethanol from Sucrose
An Introduction to Molecular Modeling
Reactivities of Some Alkyl Halides
Nucleophilic Substitution Reactions: Competing Nucleophiles
Synthesis of n-Butyl Bromide and t-Pentyl Chloride
Methyl Stearate from Methyl Oleate
Preparation of Soap1
Gas-Chromatographic Analysis of Gasolines
Chiral Reduction of Ethyl Acetoacetate; Optical Purity Determination
Nitration of Aromatic Compounds Using a Recyclable Catalyst
Resolution of (±)-a-Phenylethylamine and Determination of Optical Purity
An Oxidation-Reduction Scheme: Borneol, Camphor, Isoborneol
Multistep Reaction Sequences: The Conversion of Benzaldehyde to Benzilic Acid
Triphenylmethanol and Benzoic Acid
Aqueous-Based Organozinc Reactions
Sonogashira Coupling of lodosubstituted Aromatic Compounds with Alkynes Using a Palladium Catalyst
Grubbs-Catalyzed Metathesis of Eugenol with 1,4-Butenediol to Prepare a Natural Product
The Aldol Condensation Reaction: Preparation of Benzalacetophenones (Chalcones)
Preparation of an a, B -Unsaturated Ketone via Michael and Aldol Condensation Reactions
Relative Reactivities of Several Aromatic Compounds
Nitration of Methyl Benzoate
Preparation of Methyl Orange
Preparation of Indigo1
N,N-Diethyl-m-toluamide: The Insect Repellent "OFF"
Sulfa Drugs: Preparation of Sulfanilamide
Preparation and Properties of Polymers: Polyester, Nylon, and Polystyrene
Ring-Opening Metathesis Polymerization (ROMP) Using a Grubbs Catalyst: A Three-Step Synthesis of a Polymer
The Diels-Alder Reaction of Cyclopentadiene with Maleic Anhydride
Photoreduction of Benzophenone and Rearrangement of Benzopinacol to Benzopinacolone
Preparation of a C-4 or C-5 Acetate Ester
Friedel-Crafts Acylation
Synthesis of Substituted Chalcones: A Guided-Inquiry Experience
Green Epoxidation of Chalcones
Cyclopropanation of Chalcones
How to Find Data for Compounds: Handbooks and Catalogs
Measurement of Volume and Weight
Heating and Cooling Methods
Reaction Methods
Physical Constants of Solids: The Melting Point
Crystallization: Purification of Solids
Extractions, Separations, and Drying Agents
Physical Constants of Liquids: The Boiling Point and Density
Simple Distillation
Fractional Distillation, Azeotropes
Vacuum Distillation, Manometers
Steam Distillation
Column Chromatography
Thin-Layer Chromatography
High-Performance Liquid Chromatography (HPLC)
Gas Chromatography
Infrared Spectroscopy
Nuclear Magnetic Resonance Spectroscopy (Proton NMR)
Guide to the Chemical Literature
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